Abstract
31P n.m.r. studies indicate that in the Mitsunobu
reaction, alcohols react with diethyl azodicarboxylate and triphenylphosphine
in tetrahydrofuran to produce phosphorane intermediates. Diethyl
azodicarboxylate and tributylphosphine, however, result in the formation of
oxyphosphonium salt intermediates.
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53 articles.
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