Abstract
Reaction of
cholesta-2,4-dien-6-one (1) with hydrazoic acid gave cholest-4-ene-3,6-dione
(2), 6-aza-B-homocholest-2,4-dien-7-one (3), and 6-aza-B-homocholest-4-ene-3,7-dione
(4). The structures of these compounds have been established by their spectral
properties and comparison with available authentic samples. It is shown that
neither (2) nor (3) is the precursor of (4).
Cited by
4 articles.
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