Abstract
The gas chromatographic
elution behaviour is reported for a total of 16 vanadium(111) and oxovanadium(1V) fluorinated β-diketonates
on a column consisting of a lightly loaded, non-polar stationary phase and
diatomite support. The superiority of the vanadium(111) chelates is shown to include
electron-capture detection. Detection limits of 14 chelates are given for the
flame ionization detector. Separation of the two oxidation states of a metal by
gas-liquid chromatography is demonstrated for the first time.
Cited by
13 articles.
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