Abstract
A series of terminal
dicarboxylic acids, malonic acids and branched-chain aliphatic acids on
oxidation with TiC13/H2O2 in a flow system
give rise to e.s.r. spectra arising from mixtures of
radicals. In most cases the dominant radical is that formed by abstraction of
hydrogen from the β-carbon.
Malonic acids complex with titanium(III) ions sufficiently strongly to be
examined at elevated pH values without the need for added ethylenediaminetetraacetic
acid.
Cited by
26 articles.
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