1. Pacific Northwest National Laboratory, P.O. Box 999, Richland, Washington 99352 (S.W.S., T.J.J., R.L.S.); and National Institute of Standards and Technology, Analytical Chemistry Division, 100 Bureau Drive, Stop 8393, Gaithersburg, Maryland 20899-8393 (P.M.C., G.C.R., P.A.J.)