In situ Monitoring of Emulsion Polymerization using Fiber-Optic Raman Spectroscopy-Reference-Cited by-同舟云学术

In situ Monitoring of Emulsion Polymerization using Fiber-Optic Raman Spectroscopy

Published:1992-11 Issue:11 Volume:46 Page:1729-1731
ISSN:0003-7028
Container-title:Applied Spectroscopy
language:en
Short-container-title:Appl Spectrosc

Author:

Wang Chao¹,Vickers Thomas J.¹,Schlenoff Joseph B.¹,Mann Charles K.¹

Affiliation:

1. Department of Chemistry, Florida State University, Tallahassee, Florida 32306-3006

Abstract

The feasibility of a direct quantitative analysis of styrene by Raman spectroscopy during an emulsion polymerization is examined. A dispersive spectrometer fitted with an intensified diode array detector is used with excitation from the 514.5-nm line of an Ar-ion laser. The limits of detection are 0.26 weight percent styrene in the reaction mixture. Raman measurements are compared with those obtained by UV absorption measurements on extracted samples and found to give essentially the same results.

Publisher

SAGE Publications

Subject

Spectroscopy,Instrumentation

Link

http://journals.sagepub.com/doi/pdf/10.1366/0003702924926961

Reference5 articles.

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5. Schrader B., Raman/Infrared Atlas of Organic Compounds (VCH Publishers, New York, 1989), p. N03.

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