The Determination of Impurities in Plutonium Metal by Anion Exchange and ICP/AES-Reference-Cited by-同舟云学术

The Determination of Impurities in Plutonium Metal by Anion Exchange and ICP/AES

Published:1989-02 Issue:2 Volume:43 Page:223-226
ISSN:0003-7028
Container-title:Applied Spectroscopy
language:en
Short-container-title:Appl Spectrosc

Author:

Huff Edmund A.¹,Bowers Delbert L.¹

Affiliation:

1. Analytical Chemistry Laboratory, Chemical Technology Division, Argonne National Laboratory, 9700 South Cass Avenue, Argonne, Illinois 60439

Abstract

The determination of trace-metal impurities in plutonium metal was investigated with the use of anion exchange separation and analysis by inductively coupled plasma/atomic emission spectrometry. Data on recoveries and independent measurements for some 30 elements show precisions and accuracies in the 1–10% range, values that are a significant improvement over those of traditional carrier distillation techniques. Americium can be determined on the same sample aliquot, with figures of merit rivaling those of nuclear counting procedures.

Publisher

SAGE Publications

Subject

Spectroscopy,Instrumentation

Link

http://journals.sagepub.com/doi/pdf/10.1366/0003702894203318

Reference10 articles.

1. Analytical Chemistry of Plutonium

2. Ion Exchange Spectrographic Method for Determination of Impurities in Uranium and Plutonium

3. The spectrographic analysis of plutonium for twenty-two trace impurities by the D.C. arc method

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