FT-Raman Microscopy: Discussion and Preliminary Results

Author:

Messerschmidt Robert G.1,Chase D. Bruce1

Affiliation:

1. Spectra-Tech, Inc., 652 Glenbrook Road, Stamford, Connecticut 06906 (R.G.M.); and E. I. DuPont deNemours, Experimental Station E-328, Wilmington, Delaware 19898 (D.B.C.)

Abstract

This paper reports on the first spectra obtained using a microscope apparatus to perform FT-Raman spectroscopy. It is considered desirable to use a standard FT-IR microscope for these measurements, since this approach may lead to the attainment of both FT-IR and FT-Raman microscope data from a single instrument. The relative performance of the microscope apparatus compared to that of a previously designed macro-apparatus is studied. The described micro-apparatus is then used to measure the FT-Raman spectrum of a single crystal of bis-methyl-styry I benzene and of a single fiber of Kevlar®. The results indicate an acceptable sensitivity, for these small samples.

Publisher

SAGE Publications

Subject

Spectroscopy,Instrumentation

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