Preparation and Crystal Structure of a New Lithium Vanadium Fluoride Li2VF6 with Trirutile-type Structure-Reference-Cited by-同舟云学术

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Preparation and Crystal Structure of a New Lithium Vanadium Fluoride Li2VF6 with Trirutile-type Structure

Published:2013-02-01 Issue:2 Volume:68 Page:121-126
ISSN:1865-7117
Container-title:Zeitschrift für Naturforschung B
language:en
Short-container-title:

Author:

Nakhal Suliman¹,Weber Dominik¹,Lerch Martin¹

Affiliation:

1. Institut für Chemie, Technische Universität Berlin, Straße des 17. Juni 135, D-10623 Berlin, Germany

Abstract

A new lithium vanadium fluoride Li2VF6 was prepared by reacting lithium fluoride LiF with vanadium tetrafluoride VF4 in a monel capsule at 500 °C. The crystal structure has been determined by means of powder X-ray diffraction. Trirutile-type dilithium hexafluorovanadate(IV) crystallizes in the tetragonal space group P42/mnmwith lattice parameters a=459.99(1), b=459:99(1), c=896.64(2) pm. The presence of a Jahn-Teller effect is discussed.

Publisher

Walter de Gruyter GmbH

Subject

General Chemistry

Link

https://www.degruyter.com/document/doi/10.5560/znb.2013-2303/pdf

Cited by 2 articles. 订阅此论文施引文献订阅此论文施引文献，注册后可以免费订阅5篇论文的施引文献，订阅后可以查看论文全部施引文献

1. Exploratory Synthesis for Complex Metal Fluorides Using Solid-State Fluorine Sources;Inorganic Chemistry;2022-01-12

2. ChemInform Abstract: Preparation and Crystal Structure of a New Lithium Vanadium Fluoride Li2VF6with Trirutile-Type Structure.;ChemInform;2013-05-02

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