An Efficient Multicomponent Synthesis of Octahydroquinazolinone Derivatives Using Novel Recyclable Grafted Fe APA-Complex Catalyst
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Published:2018-11-19
Issue:
Volume:
Page:30-35
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ISSN:2394-4099
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Container-title:International Journal of Scientific Research in Science, Engineering and Technology
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language:en
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Short-container-title:IJSRSET
Author:
Sangle S. L.1, Ghumare S. S.1
Affiliation:
1. Department of Chemistry, MVP Samaj’s Arts, Science and Commerce College, Saikheda, Maharashtra, India
Abstract
Recoverable and recyclable heterogeneous grafted Fe-APA complex efficiently catalyzed the one-pot synthesis of octahydroquinazolinone derivatives via multicomponent reaction of dimedone, aromatic aldehyde, and urea using methanol as a solvent. The desired products were obtained with 84–96 % yields. The present approach offers several significants such as short reaction time, high yield, easy purification, minimum catalyst loading, and use as an alternative catalyst. Grafted Fe APA complex were synthesized and characterized by various analytical investigative techniques like FTIR, NMR, Mass, XRD, SEM, EDAX, TEM with SAED, and BET surface area.
Publisher
Technoscience Academy
Reference53 articles.
1. K Gupta, A. Sutar, Coordination Chemistry Reviews, 2008, 252, 1420. 2. L Kathryn, K. Franz, Chem.Rev, 2007, 109, 4921. 3. S Kumar, D. Dhar, P. Saxena, Journal of Scientific & Industrial Research, 2009, 68, 181. 4. E Keskioglu, A. Gunduzalp, S. Cete, F. Hamurcu, B. Erk, Spectrochim.Acta, 2008, 70A, 634. 5. M Dul, E. Pardo, R. Lescouezec, Y. Journaux, J. Ferrando-Soria, R. Ruiz-García, J. Cano, M. Julve, F. Lloret, D. Cangussu, C. L. M. Pereira, H. Stumpf, J. Pasan, C. Ruiz-Perez, Coordination Chemistry Reviews,2010, 254,228.
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