Polymorphism of Nicotinamide Riboside Chloride and Crystal Structure Determination of the Most Stable Crystalline Form

Author:

Wu Dedong1,Wu Branden2,Wei Pingrong3

Affiliation:

1. AstraZeneca (United States)

2. Newton South High School

3. University of Georgia

Abstract

Abstract Three crystalline forms of nicotinamide riboside chloride (NR-Cl), namely Form A, Form B and Form C, were prepared and characterized. Form A and Form B are true polymorphs of anhydrous forms, while Form C is a pseudo-polymorph of a methanolate solvate form. Physical stability relationship among these three crystalline forms was established, and the crystal structure of the most stable form, Form B, was determined by single crystal X-ray diffraction analysis.

Publisher

Research Square Platform LLC

Reference21 articles.

1. Nicotinamide riboside, a trace nutrient in foods, is a Vitamin B3 with effects on energy metabolism and neuroprotection;Chi Y;Curr Opin Clin Nutr Metab Care,2013

2. Chronic nicotinamide riboside supplementation is well-tolerated and elevates NAD + in healthy middle-aged and older adults;Martens CR;Nat Commun,2018

3. Nicotinamide Riboside—The Current State of Research and Therapeutic Uses;Mehmel M;Nutrients,2020

4. Szczepankiewicz B, Koppetsch K, Perni RB (2015) Preparation and use of crystalline beta-d-nicotinamide riboside. GlaxoSmithKline, p WO2015186068

5. Carlson EC, Standen MC, Morrill WM (2016) Crystalline form of nicotinamide riboside. W. R. Grace & Co. WO2016014927

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