Flow reactor experiments of high-temperature graphite oxidation and nitridation

Author:

Anderson Nicholas A.1,Zolfaghari Philip1,Bhattacharya Souvik1,Capponi Lorenzo1,Oldham Trey1,Sankaran R. Mohan1,Elliott Gregory S.1,Panerai Francesco1

Affiliation:

1. University of Illinois Urbana-Champaign

Abstract

Abstract

Predicting the gas-surface interactions of solid carbon is necessary for the design of many engineering systems that employ graphite. Experimental determination of the reaction rates improves the fidelity of those predictions. Here, we study oxidation and nitridation of graphite by thermal and non-thermal, plasma assisted processes. Experiments are conducted at a pressure of 2 kPa, higher than previous flow reactor experiments of this kind and closer to the conditions experienced in engineering applications. At these higher pressures, the limitations of mass transport and the interference between oxygen and nitrogen species become important. Reaction rates are determined from mass loss, reaction products are identified with mass spectrometry, and surface roughening is characterized by electron microscopy.

Publisher

Springer Science and Business Media LLC

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