Production of tib2 coatings on graphite substrates by electrophoretic deposition in NaF-AlF3 melt

Author:

Zhang Jun1,Pang Jie2,Jin Weiliang2,Chu Shaojun3,Haarberg Martin4,Xiao Saijun2

Affiliation:

1. School of Metallurgy Engineering, Anhui University of Technology, Yushan District, Maanshan, China + School of Metallurgical and Ecological Engineering, University of Science and Technology Beijing, Haidian District, Beijing. China

2. School of Metallurgy Engineering, Anhui University of Technology, Yushan District, Maanshan, China

3. School of Metallurgical and Ecological Engineering, University of Science and Technology Beijing, Haidian District, Beijing, China

4. Department of Materials Science and Engineering, Norwegian University of Science and Technology, Trondheim, Norway

Abstract

In this paper a novel method for fabrication of TiB2 coatings on graphite substrates by electrophoretic deposition of TiB2 nanoparticles in NaF-AlF3 melt at 980?C has been explored. With an applied cell voltage of 1.2 V (i.e. electric field 0.6 V/cm), a flat and dense TiB2 coating with a thickness of around 50 ?m has been prepared. It was found that the surface consisted of TiB2 flakes with a nanoscale size. In addition, the average value of hardness of the TiB2 coating was determined as 3585 ? 139 HV0.1 (36.6 ? 1.4GPa) measured by a Vickers micro-hardness tester.

Publisher

National Library of Serbia

Subject

Ceramics and Composites

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