Quechers approach to the Alternaria mycotoxins detection in wheat: The recovery study-Reference-Cited by-同舟云学术

Quechers approach to the Alternaria mycotoxins detection in wheat: The recovery study

Published:2022 Issue:142 Volume: Page:31-38
ISSN:0352-4906
Container-title:Zbornik Matice srpske za prirodne nauke
language:en
Short-container-title:Zb Mat srp prir nauk

Author:

Bursic Vojislava¹^ORCID,Vukovic Gorica²^ORCID,Stojanovic Tijana¹^ORCID,Marinkovic Dusan¹,Puvaca Nikola³^ORCID,Petrovic Aleksandra¹^ORCID,Konstantinovic Bojan¹^ORCID,Popov Milena¹^ORCID,Samardzic Natasa¹

Affiliation:

1. University of Novi Sad, Faculty of Agriculture, Department of Plant and Environmental Protection, Novi Sad, Serbia

2. Field Test Lht., Belgrade, Serbia

3. University Business Academy in Novi Sad, Faculty of Economics and Engineering Management in Novi Sad, Department of Engineering Management in Biotechnology, Novi Sad, Serbia

Abstract

The performance of the QuEChERS extraction followed by the LC-MS/ MS analytical method was evaluated in terms of Alternaria mycotoxins recovery from the wheat. The alternariol (AOH), tentoxin (TEN) and alternariol monomethyl ether (AME) were analyzed using the ESI+ (electrospray positive ionization) by multiple reactions mon?itoring mode (MRM). In order to determine the recovery, the blank wheat samples were spiked at two spiking levels (0.01 and 0.1 mg/kg) in six replicates. The obtained average recoveries and precisions (expressed as the RSDr, %) were as follows: 107.6% (RSDr of 6.84%) for alternariol, 108.0% (RSDr of 6.78%) for tentoxin and 110.1% (RSDr of 6.50%) for alternariol monomethyl ether. The results of this study were in accordance with the Commission Decision 2002/657/EC and Commission Regulation (EC) No 401/2006.

Publisher

National Library of Serbia

Subject

General Medicine

Reference11 articles.

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2. Commission Decision 2002/657/EC implementing Council Directive 96/23/EC concerning the performance of analytical methods and the interpretation of results.

3. Commission Regulation (EC): No 401/2006 laying down the methods of sampling and analysis for the official control of the levels of mycotoxins in foodstuffs.

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