Superalloy/Al2O3 type composite compacts obtained by spark plasma sintering from mechanically alloyed powders

Author:

Prică Călin1,Sechel Niculina1,Neamțu Bogdan1,Marinca Traian1,Popa Florin1,Chicinaș Horea1,Chicinaș Ionel1

Affiliation:

1. Materials Science and Engineering Department, Technical University of Cluj-Napoca, Cluj-Napoca, Romania

Abstract

Fe-base Superalloy/Al2O3 type composite compacts were successfully obtained by spark plasma sintering from mechanically alloyed powders. The superalloy powders without Al2O3 and superalloy/Al2O3 type composites powders with 5 and 10 %vol. Al2O3 were synthesized from elemental powders in a high energy planetary mill. The influence of the milling process on particle size evolution has been determined using a Laser Particle Size Analyzer with an analysis field of 0.1-1000 ?m. The composite compacts were obtained by spark plasma sintering. Both, composite powders, and compacts were investigated by X-ray diffraction (XRD), high temperature X-ray diffraction (HT-XRD), scanning electron microscopy (SEM) and energy dispersive X-ray spectroscopy (EDX).

Publisher

National Library of Serbia

Subject

Materials Chemistry,Metals and Alloys,Condensed Matter Physics,Ceramics and Composites

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