Author:
Ling Jie,Li Xiao,Wang Maolin,Zhang Chaozheng,Liu Yilan,Zhang Xin,Liu Changqun,Ren Qing,Zeng Yingjie,Wang Chuanqi,Chen Ying,Sun Chen,Chen Hongyu,Zuo Yi,Deng Yun,Cao Xiujun,Ren Bo,Li Defang,Lu Jun
Reference113 articles.
1. After stirring at room temperature for 3 h, the reaction was finished by TLC indication. The mixture was quenched with a hydrochloric acid solution (1 N, 3�10 mL), extracted with DCM (3�30 mL), dried over anhydrous sodium sulfate, and filtered. The solvent was removed under reduced pressure. The residue was purified by column chromatography using DCM;Compound 2 was dissolved in DCM (5 mL), followed by adding ethanolamine (27 ?L, 0.21 mmol), pyridine (13 ?L, 0.14 mmol), and DMAP (3 mg, 0.02 mmol)