Synthesis of nanostructured zirconium monosilicide via a lithium thermal reduction route at low temperature

Author:

Wang Liangbiao1,Yang Ting-Hai1,Chen Zhe2,Zhou Ziming2,Li Qianwen3,Gong Huaxu2,Zhang Kailong4,Du Qinyi2,Xin Yan2,Huang Zixun2

Affiliation:

1. School of Chemistry and Environment Engineering Jiangsu University of Technology No. 1801 Zhongwu Road Changzhou 213001, China

2. School of Chemistry and Environment Engineering, Jiangsu University of Technology, Changzhou , China

3. College of Light-Textile Engineering and Art, Anhui Agriculture University, Hefei , China

4. National & Local Joint Engineering Research Center for Deep Utilization Technology of Rock-salt Resource, Faculty of Chemical Engineering, Huaiyin Institute of Technology, Huaian , China

Abstract

Abstract In this paper, orthorhombic phase zirconium monosilicide nanomaterials have been successfully synthesized through a lithium thermal reduction in a stainless-steel autoclave at a low temperature of 600 0C. X-ray diffraction indicates that the obtained product is orthorhombic zirconium monosilicide. Scanning electron microscopy shows that the obtained zirconium monosilicide product consists of nanoparticles and nanorods. The oxidation resistance of the obtained zirconium monosilicide product is investigated.

Publisher

Walter de Gruyter GmbH

Subject

Materials Chemistry,Metals and Alloys,Physical and Theoretical Chemistry,Condensed Matter Physics

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