Deposition of Multilayer Films of ZnO by Sol-gel Process on Stainless Steel Substrates for Energy Harvesting Devices

Abstract

Abstract The mechanical vibrations surrounding the environment can be converted in electrical energy by piezoelectric energy harvesters (PEH). The increase on the availability of Wireless Sensor Networks (WSN) increases the need for power supply that replaces ordinary batteries. In this paper, an electromechanical modelling and a deposition of multilayer zinc oxide (ZnO) films for an PEH are presented. The aim of the study is to obtain the thickness of the multilayer ZnO films in different conditions, in order to improve the energy harvesting capacity for a PEH device. The ZnO synthesis was performed by the sol-gel method with dehydrated zinc acetate as a precursor, making deposits of 5, 10 and 15 layers. The depositions were made at room temperature by spin coating at 1440 revolutions per minute for 16 s. An UV-Vis test showed that ZnO were present, with a percentage of peak reflectance at 370 nm and a XRD test showed a preferential crystalline orientation at (002). Also, a Finite Element Modelling (FEM) simulation of the substrate behaviour was performed, functioning as a cantilever beam. When adding a seismic mass and oscillating in the resonance frequency of 103.31 Hz and with 15 layers of ZnO deposited, 2.67 volts were obtained.