Nickel oxide reduction in CO/CO2 gas mixtures in reverberatory furnaces

Abstract

Abstract This study present laboratory experiments carried out for nickel oxide reduction in a reverberatory furnace at medium pressure and a temperature range of 400˚C-1050˚C. Analyses were carried out on nickel nanostructures and their partially reduced metallic nickel products using Zeiss Leo Supra 35 SEM. It became evident from the experimental processes that the reduction process of nickel oxide under those given pressure and temperature conditions can result in fractionation of a dense layer of nickel from the melt surface which is in association with continuous growth of gaseous pores in nickel oxide. Therefore thermodynamic processes and temperature conditions are regarded as the most important factors which play a fundamental role in the reduction process of nickel oxide (gas-metal, or/and oxide-metal). The results indicate a positive correlation between formation mechanism and the rate of reduction of metallic nickel phases upon inter. Our research took a step-by-step assessment of technological processes and a scientific observation on nickel reduction at chemical equilibrium state of an ideal gas was made, and an account was taken with regards to limitations of variables and melting parameters.