Strategies to minimize beam and sample vibration-induced instabilities at the microfocus MX XAIRA beamline at ALBA

Abstract

Abstract The performance of microfocus beamlines, and ultimately the quality of the diffraction data, is very sensitive to vibrations affecting the optical elements and the sample stages and holder. We report here the strategies applied in the design of the microfocus MX XAIRA beamline at ALBA synchrotron to mitigate the effects of two relevant sources of vibrations: circulation of LN2 flow to evacuate the thermal load on the monochromator and cryocooling gas stream being blown on the sample. The internal shape and size of the two cooling pads that clamp the monochromator optics have been designed to minimize the turbulences in the liquid nitrogen flow while maximizing heat transfer. Computational Fluid Dynamics (CFD) simulations and some preliminary metrology tests are presented. Besides, in the end-station, the cryo-cooler is blowing typically a 5-10 L/min flow of nitrogen or helium gas at 100K on the sample, inducing vibrations in the micron range. The optimal geometrical configuration between the sample holder and the cryocooler has been assessed by means of CDF simulations and metrology tests.