Author:
Cervera M. Luisa,Lopez J. Carlos,Montoro Rosa
Abstract
SummaryThe arsenic content of cows' milk consumed in Spain was determined. A procedure using dry ashing hydride generation atomic absorption spectrometry was developed for the purpose. Experimental conditions for the destruction of organic matter were established and an interference study was carried out. The method developed has a detection limit of 0·1 ng/g, a relative SD of 5%, and a recovery (mean ± CSI) of 100 ± 4%. The accuracy of the method was checked by analysis of a certified sample of IAEA milk powder (mean ± CSI: certified, 4·85 ± 0·32 ng/g; found, 5·04 ± 0·81 ng/g). The proposed procedure was used to analyse cows' milk samples. The extremely low arsenic levels found do not present toxicological problems.
Publisher
Cambridge University Press (CUP)
Subject
Animal Science and Zoology,General Medicine,Food Science
Reference24 articles.
1. Dry ashing, hydride generation atomic absorption spectrometric determination of arsenic and selenium in foods;Tam;Journal of the Association of Official Analytical Chemists,1982
2. Hydride generation atomic absorption determination of arsenic in marine sediments, tissues and sea water with in situ concentration in a graphite furnace
3. Determination of arsenic and selenium in fat materials and petroleum products by oxygen bomb combustion and automated atomic absorption spectrometry with hydride generation
4. Arsenic in Dutch milk powder. Determination by atomic absorption spectroscopy after cold trapping of the generated hydride;Koops;Netherlands Milk and Dairy Journal,1989
Cited by
21 articles.
订阅此论文施引文献
订阅此论文施引文献,注册后可以免费订阅5篇论文的施引文献,订阅后可以查看论文全部施引文献