14C Measurements of Sub-Milligram Carbon Samples from Aerosols

Author:

Weissenbök Roland,Biegalski Steven R.,Currie Lloyd A.,Klinedinst Donna B.,Golser Robin,Klouda George A.,Kutschera Walter,Priller Alfred,Rom Werner,Steier Peter,Wild Eva

Abstract

Accelerator mass spectrometry (AMS) at the milligram level is routinely performed, but it is difficult to go substantially below 100 μg of carbon. We discuss various approaches for sample preparation, machine operation and data evaluation, to meet the special requirements of 14C AMS measurements at the microgram-carbon level. Furthermore, we present first results obtained at the Vienna Environmental Research Accelerator (VERA) from 14C measurements of a snow sample from Gaithersburg, Maryland, USA, prepared at the National Institute of Standards and Technology (NIST).

Publisher

Cambridge University Press (CUP)

Subject

General Earth and Planetary Sciences,Archeology

Cited by 9 articles. 订阅此论文施引文献 订阅此论文施引文献,注册后可以免费订阅5篇论文的施引文献,订阅后可以查看论文全部施引文献

1. Accelerator Mass Spectrometry Targets of Submilligram Carbonaceous Samples Using the High-Throughput Zn Reduction Method;Analytical Chemistry;2009-06-23

2. Microgram level radiocarbon (14C) determination on carbonaceous particles in ice;Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms;2007-06

3. Progress in isotope analysis at ultra-trace level by AMS;International Journal of Mass Spectrometry;2005-04

4. THEODORE, a two-step heating system for the EC/OC determination of radiocarbon (14C) in the environment;Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms;2004-08

5. Technical progress in AMS microscale radiocarbon analysis;Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms;2004-08

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