1H-and 13C-n.m.r. spectroscopy of 2-oxo-3-deoxy-d-glycero-d- galactononulosonic acid-containing oligosaccharide-alditols bearing Lewis X, Lewis Y and A-Lewis Y determinants isolated from the jelly coat of Pleurodeles waltl eggs-Reference-Cited by-同舟云学术

1H-and 13C-n.m.r. spectroscopy of 2-oxo-3-deoxy-d-glycero-d- galactononulosonic acid-containing oligosaccharide-alditols bearing Lewis X, Lewis Y and A-Lewis Y determinants isolated from the jelly coat of Pleurodeles waltl eggs

Published:1992-11-01 Issue:3 Volume:287 Page:905-909
ISSN:0264-6021
Container-title:Biochemical Journal
language:en
Short-container-title:

Author:

Strecker G¹,Wieruszeski J M¹,Michalski J C¹,Montreuil J¹

Affiliation:

1. Laboratoire de Chimie Biologique et Unité Mixte de Recherche du CNRS 111, Université des Sciences et Technologies de Lille, Lille, 59655 Villeneuve d'Ascq Cedex, France.

Abstract

Three acidic oligosaccharide-alditols carrying Lewis X, Lewis Y and A-Lewis Y determinants were isolated from the jelly coat of Pleurodeles waltl eggs. These compounds possess the following structures. Gal beta 1-4(Fuc alpha 1-3)GlcNAc beta 1-3[2-oxo-3-deoxy-D- glycero-D-galactononulosonic acid (KDN)alpha 2-6] GalNAc-ol; Fuc alpha 1-2Gal beta 1-4(Fuc alpha 1-3)GlcNAc beta 1-3(KDN alpha 2-6) GalNAc-ol and Fuc alpha 1-2(GalNAc alpha 1-3)Gal beta 1-4(Fuc alpha 1-3)GlcNAc beta 1-3(KDN alpha 2-6)GalNAc-ol. The complete 1H-n.m.r.-spectrum assignment for the three compounds and the 13C-n.m.r. analysis of the A-Lewis Y determinant-containing heptasaccharide are reported.

Publisher

Portland Press Ltd.

Subject

Cell Biology,Molecular Biology,Biochemistry

Link

https://portlandpress.com/biochemj/article-pdf/287/3/905/628907/bj2870905.pdf

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