Research of the thermal effect on the Fe–Cr–Al alloy foil in the initial state and with the deposited secondary support-Reference-Cited by-同舟云学术

Research of the thermal effect on the Fe–Cr–Al alloy foil in the initial state and with the deposited secondary support

Published:2023-03-01 Issue:3 Volume:78 Page:271-280
ISSN:0932-0784
Container-title:Zeitschrift für Naturforschung A
language:en
Short-container-title:

Author:

Khussain Bolatbek¹,Brodskiy Alexandr²,Sass Alexandr³,Teltayev Bagdat⁴,Rakhmetova Kenjegul³

Affiliation:

1. D.V. Sokolskiy Institute of Fuel, Catalysis and Electrochemistry , 050010, 142 Kunaev Str. , Almaty , Republic of Kazakhstan

2. Laboratory of Physical Research Methods , D.V. Sokolskiy Institute of Fuel, Catalysis and Electrochemistry , 050010, 142 Kunaev Str. , Almaty , Republic of Kazakhstan

3. Department of Engineering , D.V. Sokolskiy Institute of Fuel, Catalysis and Electrochemistry , 050010, 142 Kunaev Str. , Almaty , Republic of Kazakhstan

4. Kazakhstan Highway Research Institute , 050061, 2a Nurpeisov Str. , Almaty , Republic of Kazakhstan

Abstract

Abstract The purpose of this work is to study the influence of thermal effect on the surface morphology of the Fe–Cr–Al (Kh15Yu5) alloy foil and the elemental composition of the surface layers. Also, studies have been carried out on the physicochemical characteristics of the primary support with the deposited secondary support in the initial state and within the temperature range from 25 to 900 °C. The research was carried out on a JSM 6610 LV, JEOL scanning electron microscope with an installed INCA Energy 450 energy-dispersive microanalysis system. Before depositing secondary support (aluminum oxide), for a stronger adhesion to the foil metal, the foil surface was pretreated with a phosphating solution. It was found that during heating up the elemental composition of the surface layer of the Kh15Yu5-alloy foil does not remain constant and depends on the mode of thermal effect. This implies the possibility of changing the adhesion and adsorption properties of the foil surface, as well as the need to take this into account when depositing secondary support and an active phase to the foil. Studies have shown that the applied methods for phosphatizing and depositing secondary support to the foil surface make it possible to obtain a quite resistant coating. No peeling of the secondary support from the foil surface is observed during high-temperature treatment in the air.

Publisher

Walter de Gruyter GmbH

Subject

Physical and Theoretical Chemistry,General Physics and Astronomy,Mathematical Physics

Link

https://www.degruyter.com/document/doi/10.1515/zna-2022-0272/pdf

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