X-ray diffraction and Mössbauer spectroscopy studies of a mechanosynthesized Fe75B25 alloy-Reference-Cited by-同舟云学术

X-ray diffraction and Mössbauer spectroscopy studies of a mechanosynthesized Fe75B25 alloy

Published:2015-03-01 Issue:1 Volume:60 Page:43-46
ISSN:0029-5922
Container-title:Nukleonika
language:en
Short-container-title:

Author:

Jartych Elżbieta¹,Kubalova Ludmila M.²,Fadeeva Victoria I.³

Affiliation:

1. Institute of Electronics and Information Technology, Lublin University of Technology, 38A Nadbystrzycka Str., 20-618 Lublin, Poland, Tel.: +48 81 538 4618, Fax: +48 81 538 4312

2. Department of Chemistry, North Ossetian State University after K. L. Khetagurov, 44-46 Vatutina Str., 362025 Vladikavkaz, Russia

3. Department of Chemistry, M. V. Lomonosov Moscow State University, Leninsky Gory, 119899 Moscow, Russia

Abstract

Abstract In this work, the process of formation of metastable phases was investigated for the Fe75B25 composition. Mechanical synthesis was performed in a MAPF-2M high-energy planetary ball mill under an argon atmosphere. X-ray diffraction (XRD), differential scanning calorimetry (DSC), and Mössbauer spectroscopy (MS) were applied to recognize the phases. After 6 h of milling, the material consisted of two phases, that is, metastable tetragonal t-Fe2B and amorphous phases. During further thermal processing, the metastable phase was transformed into the stable Fe2B phase.

Publisher

Walter de Gruyter GmbH

Subject

Waste Management and Disposal,Condensed Matter Physics,Safety, Risk, Reliability and Quality,Instrumentation,Nuclear Energy and Engineering,Nuclear and High Energy Physics

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