Metallation of Calix[4]arene with Thulium Diiodide, TmI2(DME)3: Molecular Structure of [(5,11,17,23-Tetra-tert-butyl-25,27-dioxo-26,28- dimethoxycalix[4]arene)thulium(III)iodide(diethyl etherate)]-Reference-Cited by-同舟云学术

Metallation of Calix[4]arene with Thulium Diiodide, TmI2(DME)3: Molecular Structure of [(5,11,17,23-Tetra-tert-butyl-25,27-dioxo-26,28- dimethoxycalix[4]arene)thulium(III)iodide(diethyl etherate)]

Published:1999-04-01 Issue:4 Volume:54 Page:466-468
ISSN:1865-7117
Container-title:Zeitschrift für Naturforschung B
language:en
Short-container-title:

Author:

Fedushkin Igor L.¹,Weydert Marc²,Fagin Anatoly A.¹,Nefedov Sergei E.³,Eremenko Igor L.³,Bochkarev Mikhail N.¹,Schumann Herbert²

Affiliation:

1. G. A. Razuvaev Institute of Organometallic Chemistry of Russian Academy of Sciences, Tropinina 49, 603600 Nizhny Novgorod GSP-445 (Russian Federation)

2. Institut für Anorganische und Analytische Chemie der Technischen Universität Berlin, Straße des 17. Juni 135, D -10623 Berlin (Deutschland)

3. N. S. Kurnakov Institute of General and Inorganic Chemistry of Russian Academy of Sciences, Leninskii prospect 31,117907 Moscow GSP-1 (Russian Federation)

Abstract

[(5,11,17,23-Tetra-tert-butyl-25,27-dioxo-26,28-dimethoxycalix[4]arene)thulium(III)-iodide( diethyl etherate)] 1 is obtained by deprotonation of 5,11,17,23-tetra-tert-butyl-25,27- dihydroxy-26,28-dimethoxy-calix[4]arene with 2 equivalents of Tml2(DME)3 in THF.

Publisher

Walter de Gruyter GmbH

Subject

General Chemistry

Link

https://www.degruyter.com/document/doi/10.1515/znb-1999-0408/pdf

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