Crystal structure of 9-(2-chloroethoxy)-4-(4-methoxy-3-(trifluoromethyl)phenyl)- 5,6-dihydrobenzo[h]quinazolin-2-amine, C22H19ClF3N3O2-Reference-Cited by-同舟云学术

Crystal structure of 9-(2-chloroethoxy)-4-(4-methoxy-3-(trifluoromethyl)phenyl)- 5,6-dihydrobenzo[h]quinazolin-2-amine, C₂₂H₁₉ClF₃N₃O₂

Published:2023-01-30 Issue:2 Volume:238 Page:243-245
ISSN:1433-7266
Container-title:Zeitschrift für Kristallographie - New Crystal Structures
language:en
Short-container-title:

Author:

Li Rong-Kai¹,Wang Chun-Hua¹,Hou Gui-Ge¹^ORCID,Li Cheng-Bo¹

Affiliation:

1. School of Pharmacy, The Key Laboratory of Prescription Effect and Clinical Evaluation of State Administration of Traditional Chinese Medicine of China , Binzhou Medical University , Yantai , 264003 , P. R. China

Abstract

Abstract C22H19ClF3N3O2, triclinic, P 1 ‾

$P\overline{1}$

(no. 2), a = 9.8138(7) Å, b = 10.9739(7) Å, c = 11.6878(9) Å, α = 62.633(7)°, β = 67.095(7)°, γ = 68.817(6)°, V = 1003.78(14) Å3, Z = 2, R gt (F) = 0.0454, wR ref (F 2) = 0.1158, T = 293 K.

Publisher

Walter de Gruyter GmbH

Subject

Inorganic Chemistry,Condensed Matter Physics,General Materials Science

Link

https://www.degruyter.com/document/doi/10.1515/ncrs-2022-0589/pdf

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4. Katila, P., Shrestha, A., Shrestha, A., Shrestha, R., Park, P. H., Lee, E. S. Introduction of amino moiety enhances the inhibitory potency of 1-tetralone chalcone derivatives against LPS-stimulated reactive oxygen species production in RAW 264.7 macrophages. Bioorg. Chem. 2019, 87, 495–505; https://doi.org/10.1016/j.bioorg.2019.03.055.

5. Sun, Y., Gao, Z., Wang, C., Hou, G.-G. Synthesis, crystal structures and anti-inflammatory activity of fluorine-substituted 1,4,5,6-tetrahydrobenzo[h]quinazolin-2-amine derivatives. Acta Crystallogr. 2019, C75, 1157–1165; https://doi.org/10.1107/s2053229619010118.

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1. Crystal structure of 9-fluoro-4-(6-methoxypyridin-3-yl)-5,6-dihydrobenzo[h]quinazolin-2-amine, C₁₈H₁₅FN₄O;Zeitschrift für Kristallographie - New Crystal Structures;2023-11-07

2. Crystal structure of 2-amino-4-(2-fluoro-3-(trifluoromethyl)phenyl)-9-methoxy-1,4,5,6-tetrahydrobenzo[h]quinazolin-3-ium chloride, C₂₀H₁₈ClF₄N₃O;Zeitschrift für Kristallographie - New Crystal Structures;2023-10-11

3. Crystal structure of 2-amino-4-(2-fluoro-4-(trifluoromethyl)phenyl)-9-methoxy-1,4,5,6-tetrahydrobenzo[h]quinazolin-3-ium chloride, C₂₀H₁₈ClF₄N₃O;Zeitschrift für Kristallographie - New Crystal Structures;2023-08-11