Crystal structure of (8R,10R,14R, Z)-2-((3–Fluoropyridin-4-yl) methylene)-12-hydroxy-4,4,8,10,14-pentamethyl-17-((R)-2,6, 6-trimethyltetrahydro-2H-pyran-2-yl) hexadecahydro-3H-cyclopenta[a] phenanthren-3-one, C36H52FNO3-Reference-Cited by-同舟云学术

Crystal structure of (8R,10R,14R, Z)-2-((3–Fluoropyridin-4-yl) methylene)-12-hydroxy-4,4,8,10,14-pentamethyl-17-((R)-2,6, 6-trimethyltetrahydro-2H-pyran-2-yl) hexadecahydro-3H-cyclopenta[a] phenanthren-3-one, C36H52FNO3

Published:2021-07-30 Issue:6 Volume:236 Page:1139-1142
ISSN:1433-7266
Container-title:Zeitschrift für Kristallographie - New Crystal Structures
language:en
Short-container-title:

Author:

Zhang Mei¹,Meng Qing-Guo¹,Hou Gui-Ge²,Jiang Sheng³,Jin Yong-Sheng⁴,Gao Yue⁵

Affiliation:

1. School of Pharmacy , Collaborative Innovation Center of Advanced Drug Delivery System and Biotech Drugs in Universities of Shandong, Key Laboratory of Molecular Pharmacology and Drug Evaluation (Yantai University), Ministry of Education, Yantai University , Yantai , P. R. China

2. School of Pharmacy , The Key Laboratory of Prescription Effect and Clinical Evaluation of State Administration of Traditional Chinese Medicine of China, Binzhou Medical University , Yantai , 264003 , P. R. China

3. Shandong Wendeng Jizhen American Ginseng Industry Co., Ltd. , Shandong , 264400 , P. R. China

4. Department of Organic Chemistry, School of Pharmacy , Naval Medical University , Shanghai , 200433 , P. R. China

5. Department of Lab Teaching, School of Pharmacy , Naval Medical University , Shanghai , 200433 , P. R. China

Abstract

Abstract C36H52FNO3, orthorhombic, P212121 (no. 19), a = 7.8016(7) Å, b = 13.1609(10) Å, c = 30.536(2) Å, V = 3135.3(4) Å3, Z = 4, R gt (F) = 0.0657, wR ref (F 2) = 0.1435, T = 100 K.

Publisher

Walter de Gruyter GmbH

Subject

Inorganic Chemistry,Condensed Matter Physics,General Materials Science

Link

https://www.degruyter.com/document/doi/10.1515/ncrs-2021-0248/pdf

Reference14 articles.

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3. Sheldrick, G. M. Crystal structure refinement with SHELXL. Acta Crystallogr. 2015, C71, 3–8; https://doi.org/10.1107/s2053229614024218.

4. Sheldrick, G. M. SHELXTL – integrated space-group and crystal-structure determination. Acta Crystallogr. 2015, A71, 3–8; https://doi.org/10.1107/s2053273314026370.

5. Liu, J., Xu, Y. R., Yang, J. J., Wang, W. Z., Zhang, J. Q., Zhang, R. M., Meng, Q. G. Discovery, semisynthesis, biological activities, and metabolism of ocotillol-type saponins. J. Ginseng Res. 2017, 41, 373–378; https://doi.org/10.1016/j.jgr.2017.01.001.

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