The pseudosymmetric crystal structure of 3-((1R,2S)-1-methylpyrrolidin-1-ium-2-yl)pyridin-1-ium hexachloridostannate(IV), C10H16N2SnCl6-Reference-Cited by-同舟云学术

The pseudosymmetric crystal structure of 3-((1R,2S)-1-methylpyrrolidin-1-ium-2-yl)pyridin-1-ium hexachloridostannate(IV), C₁₀H₁₆N₂SnCl₆

Published:2022-04-18 Issue:4 Volume:237 Page:535-538
ISSN:1433-7266
Container-title:Zeitschrift für Kristallographie - New Crystal Structures
language:en
Short-container-title:

Author:

Wolke Marie Barbara¹,Reiss Guido J.¹^ORCID

Affiliation:

1. Institut für Anorganische Chemie und Strukturchemie, Lehrstuhl II: Material- und Strukturforschung, Heinrich-Heine-Universität Düsseldorf , Universitätsstrasse 1, D-40225 Düsseldorf , Germany

Abstract

Abstract C10H16N2SnCl6, monoclinic, I2 (no. 5), a = 14.0477(4) Å, b = 8.9140(2) Å, c = 27.6199(6) Å, β = 93.060(2)°, Z = 8, V = 3453.67(15) Å3, R gt (F) = 0.0395, wR ref = 0.0858, T = 290 K.

Publisher

Walter de Gruyter GmbH

Subject

Inorganic Chemistry,Condensed Matter Physics,General Materials Science

Link

https://www.degruyter.com/document/doi/10.1515/ncrs-2022-0010/pdf

Reference27 articles.

1. Oxford Diffraction. CrysAlispro (version 1.171.40.45a); Oxford Diffraction Ltd.: Oxford, UK, 2019.

2. Sheldrick, G. M. A short history of SHELX. Acta Crystallogr. 2008, A64, 112–122; https://doi.org/10.1107/S0108767307043930.

3. Sheldrick, G. M. Crystal structure refinement with SHELXL. Acta Crystallogr. 2015, C71, 3–8; https://doi.org/10.1107/S2053229614024218.

4. Hübschle, C. B., Sheldrick, G. M., Dittrich, B. ShelXle: a Qt graphical user interface for SHELXL. J. Appl. Crystallogr. 2011, 44, 1281–1284; https://doi.org/10.1107/S0021889811043202.

5. Parsons, S., Flack, H. D., Wagner, T. Use of intensity quotients and differences in absolute structure refinement. Acta Crystallogr. 2013, B69, 249–259; https://doi.org/10.1107/S2052519213010014.