Synthesis and crystal structure of the novel chiral acetyl-3-thiophene-5-(9-anthryl)-2-pyrazoline, C23H18N2OS

Author:

Usman Rabia1,Khan Arshad12ORCID,Refat Moamen S.3,He Nongyue12

Affiliation:

1. State Key Laboratory of Bioelectronics, National Demonstration Center for Experimental Biomedical Engineering Education, Southeast University , Nanjing 210096 , P. R. China

2. School of Materials Science and Engineering , Hunan University , Changsha 110016 , P. R. China

3. Department of Chemistry , College of Science, Taif University , P. O. Box 11099 , Taif 21944 , Saudi Arabia

Abstract

Abstract C23H18Cl4N2OS, orthorhombic, P212121 (no. 19), a = 16.872(3) Å, b = 10.414(2) Å, c = 10.589(2) Å, V = 1860.5(6) Å3, Z = 4, R gt (F) = 0.0588, wR ref (F 2) = 0.1464, T = 293 K.

Publisher

Walter de Gruyter GmbH

Subject

Inorganic Chemistry,Condensed Matter Physics,General Materials Science

Reference15 articles.

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3. Sheldrick, G. M. Crystal structure refinement with Shelxl. Acta Crystallogr. 2015, C71, 3–8; https://doi.org/10.1107/s2053229614024218.

4. Brandenburg, K. DIAMOND. Visual Crystal Structure Information System. Ver. 4.0; Crystal Impact: Bonn, Germany, 2015.

5. Usman, R., Khan, A., Wang, M. Study of H-bonded assemblies of the solvates of anthracene derivatives: guest effect on the crystal symmetry and spectroscopic properties. Supramol. Chem. 2017, 29, 497–505; https://doi.org/10.1080/10610278.2017.1284324.

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