Affiliation:
1. School of Chemistry and Materials Science , Hengyang Normal University Hengyang , Hunan 421008 , China
Abstract
Abstract
C
68
H
54
N
4
O
9
P
b
2
${\mathrm{C}}_{68}{\mathrm{H}}_{54}{\mathrm{N}}_{4}{\mathrm{O}}_{9}{\mathrm{P}\mathrm{b}}_{2}$
, monoclinic, C2/c (no. 15), a = 15.7286(14) Å, b = 16.3623(14) Å, c = 22.500(2) Å, β =
97.369
(
1
)
°
$97.369(1){}^{\circ}$
, V = 5742.7(9)
Å
3
${\mathrm{\mathring{\text{A}}}}^{3}$
, Z = 4,
R
g
t
${R}_{gt}$
(F) = 0.0203, w
R
r
e
f
${R}_{ref}$
(
F
2
${F}^{2}$
) = 0.0488, T = 296(2) K.
Funder
Hunan Provincial Natural Science Foundation
College Students Innovation and Entrepreneurship Training Program of Hunan Province
Science and Technology Plan Project of Hengyang City
Subject
Inorganic Chemistry,Condensed Matter Physics,General Materials Science
Reference11 articles.
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2. Sheldrick, G. M. SHELXTL – integrated space-group and crystal-structure determination. Acta Crystallogr. 2015, A71, 3–8.
3. Sheldrick, G. M. Crystal structure refinement with SHELXL. Acta Crystallogr. 2015, C71, 3–8; https://doi.org/10.1107/s2053229614024218.
4. Brandenburg, K. DIAMOND. Visual Crystal Structure Information System (Ver. 4.0); Crystal Impact: Bonn, Germany, 2015.
5. Sarma, R., Jubaraj, B., Baruah, J. B. Solvent coordination in changing dimensionality of lead benzoate coordination polymers. Inorg. Chim. Acta 2009, 362, 4977–4984; https://doi.org/10.1016/j.ica.2009.07.032.
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