The crystal structure of fac-tricarbonyl (N′-benzoyl-N,N-diphenylcarbamimidothioato-κ2
S,O)-(pyrazole-κN)rhenium(I) — methanol (1/1) C26H23O4N4SRe
Author:
Komane Wesley K.1ORCID, Mokolokolo Pennie2, Vatsha Banele3, Manicum Amanda-Lee E.1
Affiliation:
1. Department of Chemistry , Tshwane University of Technology , Pretoria , 0001 , South Africa 2. Department of Chemistry , University of the Free State , Bloemfontein , 9301 , South Africa 3. Department of Chemistry , University of Johannesburg , Auckland Park , 2006 , South Africa
Abstract
Abstract
C26H23O4N4SRe, triclinic, P
1
‾
$\bar{1}$
(no. 2), a = 9.919(2) Å, b = 11.752(3) Å, c = 12.717(3) Å, α = 111.098(7)°, β = 94.467(7)°, γ = 98.295(7)°, V = 1354.9(5) Å3, Z = 2, Rgt
(F) = 0.0342, wRref
(F
2) = 0.0843, T = 102.0(2) K.
Publisher
Walter de Gruyter GmbH
Subject
Inorganic Chemistry,Condensed Matter Physics,General Materials Science
Reference15 articles.
1. Bruker. SAINT–Plus (version7. 12) and SADABS (Version 2004/1); Bruker AxS Inc.: Madison, Wisconsin, USA, 2004. 2. Altomare, A., Burla, M. C., Camalli, M., Cascarano, G. L., Giacovazzo, C., Guagliardi, A., Moliterni, A. G. G., Polidori, G., Spagna, R. SIR97: a new tool for crystal structure determination and refinement. J. Appl. Crystallogr. 1999, 32, 115–119. 3. Dolomanov, O. V., Bourhis, L. J., Gildea, R. J., Howard, J. A. K., Puschmann, H. OLEX2: a complete structure solution, refinement and analysis program. J. Appl. Crystallogr. 2009, 42, 339–341. 4. Sheldrick, G. M. A short history of SHELX. Acta Crystallogr. 2008, A64, 112–122. 5. Brandenbug, K., Putz, H. DIAMOND. Visual Crystal Structure Information System. Ver. 3.0c; Crystal Impact GbR: Bonn, Germany, 2005.
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