Crystal structure of (5aS,6aS,8aR,9R,11aS, 11bS,13R,13aS)-1,1,8a,11a-tetramethyl-9-((S)-1-((S)-5-methyl-6-oxo-3,6-dihydro-2H-pyran-2-yl)ethyl)-3-oxo-1,7,8,8a,9,10,11,11a,11b,12,13,13a-dodecahydro-3H,6H-cyclopenta[5,6]cyclopropa[1,8a]naphtho[2,1-c]oxepin-13-yl acetate, C32H44O6-Reference-Cited by-同舟云学术

Crystal structure of (5aS,6aS,8aR,9R,11aS, 11bS,13R,13aS)-1,1,8a,11a-tetramethyl-9-((S)-1-((S)-5-methyl-6-oxo-3,6-dihydro-2H-pyran-2-yl)ethyl)-3-oxo-1,7,8,8a,9,10,11,11a,11b,12,13,13a-dodecahydro-3H,6H-cyclopenta[5,6]cyclopropa[1,8a]naphtho[2,1-c]oxepin-13-yl acetate, C₃₂H₄₄O₆

Published:2023-12-01 Issue:1 Volume:239 Page:117-120
ISSN:1433-7266
Container-title:Zeitschrift für Kristallographie - New Crystal Structures
language:en
Short-container-title:

Author:

Jian Cheng-Hong¹^ORCID,Chen Ren-Song¹,Zhang Jie-Jing¹,Zhao Chen-Liang¹,Zhao Neng-Wu¹,Ye Jiang-Hai¹

Affiliation:

1. Guizhou University of Traditional Chinese Medicine , Guiyang 550025 , P.R. China

Abstract

Abstract C32H44O6, monoclinic, P21 (no. 4), a = 12.2561 Å, b = 10.3674(4) Å, c = 23.3835(8) Å, β = 98.463°, V = 2938.85(19) Å3, Z = 2, R gt (F) = 0.0602, wRref (F 2) = 0.1537, T = 273(2) K.

Funder

General Projects Guizhou Science and Technology Department

Publisher

Walter de Gruyter GmbH

Subject

Inorganic Chemistry,Condensed Matter Physics,General Materials Science

Link

https://www.degruyter.com/document/doi/10.1515/ncrs-2023-0463/pdf

Reference14 articles.

1. Dolomanov, O. V., Bourhis, L. J., Gildea, R. J., Howard, J. A. K., Puschmann, H. OLEX2: a complete structure solution, refinement and analysis program. J. Appl. Crystallogr. 2009, 42, 339–341; https://doi.org/10.1107/s0021889808042726.

2. Bruker. APEX2, SAINT and SADABS; Bruker AXS Inc.: Madison, Wisconsin, USA, 2012.

3. Sheldrick, G. M. Crystal structure refinement with SHELXL. Acta Crystallogr. 2015, C71, 3–8; https://doi.org/10.1107/s2053229614024218.

4. Brandenburg, K. DIAMOND. Visual Crystal Structure Information System. Ver. 4.0; Crystal Impact: Bonn, Germany, 2015.

5. Chen, R. S., Ye, J. H., Luo, Y. L., Xu, C. Y., Zou, J., Zhang, J. J. Crystal structure of 1,2,3,5,13-pentamethoxy-6,7-dimethyl-1,2,3,4,4a,5,6,7,8, 13b-decahydrobenzo[3′,4′]cycloocta[1′,2′:4,5]benzo[1,2-d] [1,3]dioxole, C24H30O7. Z. Kristallogr. N. Cryst. Struct. 2023, 238, 349–351; https://doi.org/10.1515/ncrs-2022-0580.