Crystal structure of [meso-5,7,7,12,14,14,-hexamethyl-1,4,8,11-tetraazacyclotetradecane]nickel(II) diperchlorate – dimethylsulphoxide (1/2), C20H48Cl2N4NiO10S2-Reference-Cited by-同舟云学术

Crystal structure of [meso-5,7,7,12,14,14,-hexamethyl-1,4,8,11-tetraazacyclotetradecane]nickel(II) diperchlorate – dimethylsulphoxide (1/2), C20H48Cl2N4NiO10S2

Published:2021-08-13 Issue:6 Volume:236 Page:1243-1245
ISSN:1433-7266
Container-title:Zeitschrift für Kristallographie - New Crystal Structures
language:en
Short-container-title:

Author:

Rabi Saswata¹²,Dey Lucky²,Palit Debashis²,Dey Benu Kumar²,Rahman Ismail M. M.³^ORCID,Tiekink Edward R. T.⁴^ORCID,Roy Tapashi Ghosh²

Affiliation:

1. Department of Chemistry , Faculty of Engineering & Technology, Chittagong University of Engineering & Technology , Chattogram 4349 , Bangladesh

2. Department of Chemistry , Faculty of Science, University of Chittagong , Chattogram 4331 , Bangladesh

3. Institute of Environmental Radioactivity, Fukushima University , 1 Kanayagawa , Fukushima City , Fukushima 960-1296 , Japan

4. Research Centre for Crystalline Materials, School of Science and Technology, Sunway University , 47500 Bandar Sunway , Selangor Darul Ehsan , Malaysia

Abstract

Abstract C20H48Cl2N4NiO10S2, monoclinic, P21/n (no. 14), a = 8.657(2) Å, b = 15.233(4) Å, c = 11.956(3) Å, β = 102.737(2)°, V = 1537.9(7) Å3, Z = 2, R gt (F) = 0.0237, wR ref (F 2) = 0.0655, T = 93(2) K.

Publisher

Walter de Gruyter GmbH

Subject

Inorganic Chemistry,Condensed Matter Physics,General Materials Science

Link

https://www.degruyter.com/document/doi/10.1515/ncrs-2021-0291/pdf

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4. Sheldrick, G. M. Crystal structure refinement with CrystalClear. Acta Crystallogr. 2015, C71, 3–8; https://doi.org/10.1107/s2053229614024218.

5. Farrugia, L. J. WinGX and ORTEP for Windows: an update. J. Appl. Crystallogr. 2012, 45, 849–854; https://doi.org/10.1107/s0021889812029111.

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