Synthesis and crystal structure of 1-((7-hydroxy-3-(4-hydroxy-3-nitrophenyl)-4-oxo-4H-chromen-8-yl)methyl)piperidin-1-ium-4-carboxylate monohydrate, C22H22N2O9-Reference-Cited by-同舟云学术

Synthesis and crystal structure of 1-((7-hydroxy-3-(4-hydroxy-3-nitrophenyl)-4-oxo-4H-chromen-8-yl)methyl)piperidin-1-ium-4-carboxylate monohydrate, C₂₂H₂₂N₂O₉

Published:2023-11-01 Issue:6 Volume:238 Page:1215-1217
ISSN:1433-7266
Container-title:Zeitschrift für Kristallographie - New Crystal Structures
language:en
Short-container-title:

Author:

Chen Hai-Lin¹^ORCID,Li Xian¹,Yao Dong-Mei¹,Luo Ze-Ping¹,Wang Yan-Ping¹,Lan Jian-Jing¹

Affiliation:

1. School of Chemical and Biological Engineering , Hechi University , Yizhou District , Hechi , Guangxi , 546300 , P.R. China

Abstract

Abstract C22H22N2O9, monoclinic, P21/c (no. 14), a = 7.7374(3) Å, b = 29.1082(11) Å, c = 8.7595(3) Å, β = 96.853 ( 3 ) ∘

$96.853{(3)}^{\circ }$

, V = 1958.74(13) Å3, Z = 4, R gt(F) = 0.0520, wR ref (F 2) = 0.1501, T = 100 K.

Publisher

Walter de Gruyter GmbH

Subject

Inorganic Chemistry,Condensed Matter Physics,General Materials Science

Link

https://www.degruyter.com/document/doi/10.1515/ncrs-2023-0412/pdf

Reference9 articles.

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3. Sheldrick, G. M. Crystal structure refinement with SHELXL. Acta Crystallogr. 2015, C71, 3–8; https://doi.org/10.1107/s2053229614024218.

4. Sheldrick, G. M. SHELXTL – integrated space-group and crystal-structure determination. Acta Crystallogr. 2015, A71, 3–8; https://doi.org/10.1107/s2053273314026370.

5. Lv, X.-H., Liu, H., Ren, Z.-L., Wang, W., Tang, F., Cao, H.-Q. Design, synthesis and biological evaluation of novel flavone Mannich base derivatives as potential antibacterial agents. Mol. Divers. 2019, 23, 299–306; https://doi.org/10.1007/s11030-018-9873-9.

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