Crystal structure of methyl 1-(2-bromophenyl)-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole-3-carboxylate, C19H17BrN2O2-Reference-Cited by-同舟云学术

Crystal structure of methyl 1-(2-bromophenyl)-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole-3-carboxylate, C₁₉H₁₇BrN₂O₂

Published:2024-03-15 Issue:3 Volume:239 Page:491-493
ISSN:1433-7266
Container-title:Zeitschrift für Kristallographie - New Crystal Structures
language:en
Short-container-title:

Author:

Song Yanli¹,Du Mo¹,Zhu Zhoujing¹,Tang Wenqiang¹^ORCID,Tong Hongjuan¹^ORCID

Affiliation:

1. Xianyang Key Laboratory of Molecular Imaging and Drug Synthesis, School of Pharmacy , Shaanxi Institute of International Trade & Commerce , Xianyang , Shaanxi , China

Abstract

Abstract C19H17BrN2O2, orthorhombic, P212121 (no. 19), a = 9.3764(3) Å, b = 9.7644(3) Å, c = 17.9519(6) Å, V = 1643.58(9) Å3, Z = 4, Rgt (F) = 0.0270 wRref (F 2) = 0.0601, T = 170 K.

Publisher

Walter de Gruyter GmbH

Link

https://www.degruyter.com/document/doi/10.1515/ncrs-2024-0058/pdf

Reference15 articles.

1. Bruker. SAINT, APEX2 and SADABS; Bruker AXS Inc.: Madison, WI, USA, 2012.

2. Sheldrick, G. M. SHELXTL – integrated space-group and crystal-structure determination. Acta Crystallogr. 2015, A71, 3–8.

3. Sheldrick, G. M. Crystal structure refinement with SHELXL. Acta Crystallogr. 2015, C71, 3–8; https://doi.org/10.1107/s2053229614024218.

4. Dolomanov, O. V., Bourhis, L. J., Gildea, R. J., Howard, J. A. K., Puschmann, H. OLEX2: a complete structure solution, refinement and analysis program. J. Appl. Crystallogr. 2009, 42, 339–341; https://doi.org/10.1107/s0021889808042726.

5. Barik, S. The uniqueness of tryptophan in biology: properties, metabolism, interactions and localization in proteins. Int. J. Mol. Sci. 2020, 21, 8776; https://doi.org/10.3390/ijms21228776.