Crystal structure of 1–methyl-3-propyl-4-nitro-1H-pyrazole-5-carboxylic acid, C8H11N3O4-Reference-Cited by-同舟云学术

Crystal structure of 1–methyl-3-propyl-4-nitro-1H-pyrazole-5-carboxylic acid, C₈H₁₁N₃O₄

Published:2024-05-07 Issue:4 Volume:239 Page:635-637
ISSN:1433-7266
Container-title:Zeitschrift für Kristallographie - New Crystal Structures
language:en
Short-container-title:

Author:

Fang Wen-Chao¹,Liao Xiao-Fei²,Xiong Yuan-Zhen³,Zhao Ping¹,Huang Jian-Ping²⁴⁵⁶^ORCID

Affiliation:

1. College of Materials and Chemical Engineering , Southwest Forestry University , Kunming 650224 , P.R. China

2. College of Chemistry and Materials , Jiangxi Agricultural University , Nanchang 330045 , P.R. China

3. College of Pharmacy , Nanchang University , Nanchang 330031 , P.R. China

4. Key Laboratory of Chemical Utilization of Plant Resources of Nanchang , Nanchang Jiangteng Pharmaceutical Ltd , Nanchang 330045 , P.R. China

5. Jiangxi Jiren Linhua Industrial Co., Ltd , Chongren 344200 , P.R. China

6. Jiangxi Longyuan Chemical Industry Co., Ltd , Zhangshu 331200 , P.R. China

Abstract

Abstract [C8H11N3O4], monoclinic, P21/c (no. 14), a = 4.5811(16) Å, b = 19.734(7) Å, c = 11.812(4) Å, β = 101.181(11)°, V = 1047.6(6) Å3, Z = 4, Rgt (F) = 0.0742, wRref (F 2) = 0.1176, T = 296(2) K.

Funder

Natural Science Foundation of Science and Technology Department of Jiangxi Province

Science and Technology Research Project of Education Department of Jiangxi Province

Natural Science Foundation of Nanchang City

Natural Science Foundation of Fuzhou City, Jiangxi Province

Natural Science Foundation of Jiangxi Agriculture University

2021 Innovation Team Project of Ji’an City, Jiangxi Province

Publisher

Walter de Gruyter GmbH

Link

https://www.degruyter.com/document/doi/10.1515/ncrs-2024-0114/pdf

Reference14 articles.

1. Bruker. APEX2, SAINT and SADABS; Bruker AXS Inc.: Madison, Wisconsin, USA, 2009.

2. Sheldrick, G. M. A Short History of SHELX. Acta Crystallogr. 2008, A64, 112–122. https://doi.org/10.1107/s0108767307043930.

3. Sheldrick, G. M. Crystal Structure Refinement with SHELXL. Acta Crystallogr. 2015, C71, 3–8. https://doi.org/10.1107/s2053229614024218.

4. Brandenburg, K. DIAMOND. Visual Crystal Structure Information System. Ver. 4.0; Crystal Impact: Bonn, Germany, 2015.

5. Goldstein, I.; Burnett, A. L.; Rosen, R. C.; Park, P. W.; Stecher, V. J. The Serendipitous Story of Sildenafil: An Unexpected Oral Therapy for Erectile Dysfunction. Sex. Med. Rev. 2019, 7, 115–128. https://doi.org/10.1016/j.sxmr.2018.06.005.