Crystal structure of 3-[(triisopropylsilanyl)-ethynyl]-6a,12a-dihydro-1H-1,4-diaza-benzo[α]anthracene-2,7,12-trione, C27H28N2O3Si-Reference-Cited by-同舟云学术

Crystal structure of 3-[(triisopropylsilanyl)-ethynyl]-6a,12a-dihydro-1H-1,4-diaza-benzo[α]anthracene-2,7,12-trione, C27H28N2O3Si

Published:2020-08-26 Issue:5 Volume:235 Page:1129-1131
ISSN:2197-4578
Container-title:Zeitschrift für Kristallographie - New Crystal Structures
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Author:

Zhu Lei¹,Luo Na¹,Chen Jinyang²,Zhang Mingzhong²,Zhao Jingzhe¹,Miao Shaobin³

Affiliation:

1. College of Chemistry and Chemical Engineering, Hunan University, ChangSha, Hunan, 410082 China

2. College of Chemistry and Chemical Engineering, Yangtze Normal University, Fuling, Chongqing, 408000 China

3. Department of Chemistry and Physics, Augusta University, 1120 15th St., Augusta, GA 30912, USA

Abstract

AbstractC27H28N2O3Si, triclinic, P1̄ (no. 2), a = 7.5098(4) Å, b = 7.8881(4) Å, c = 20.8904(14) Å, α = 97.002(5)°, β = 98.703(5)°, γ = 95.739(5)°, V = 1205.25(12) Å3, Z = 2, Rgt(F) = 0.0586, wRref(F2) = 0.1610, T = 100(2) K.

Publisher

Walter de Gruyter GmbH

Subject

Inorganic Chemistry,Condensed Matter Physics,General Materials Science

Link

https://www.degruyter.com/downloadpdf/journals/ncrs/235/5/article-p1129.xml

Reference18 articles.

1. OLEX2: a complete structure solution, refinement and analysis program;J. Appl. Crystallogr,2009

2. One-step synthesis of dialkynyl-1, 2-diones and their conversion to fused pyrazines bearing enediyne units;Tetrahedron,1997

3. Clean preparation of S-thiocarbamates with in situ generated hydroxide in 2-methyltetrahydrofuran;Chin. Chem. Lett,1997

4. OLEX2: a complete structure solution, refinement and analysis program;J. Appl. Crystallogr,2009

5. Modification of acenes for n-channel OFET meterials;J. Mater. Chem. C,2018