Crystal structure of 2-({[5-(adamantan-2-yl)-2-sulfanylidene-1,3,4-oxadiazolidin-3-yl]methyl}amino)benzonitrile, C20H22N4OS-Reference-Cited by-同舟云学术

Crystal structure of 2-({[5-(adamantan-2-yl)-2-sulfanylidene-1,3,4-oxadiazolidin-3-yl]methyl}amino)benzonitrile, C₂₀H₂₂N₄OS

Published:2022-12-19 Issue:2 Volume:238 Page:159-161
ISSN:1433-7266
Container-title:Zeitschrift für Kristallographie - New Crystal Structures
language:en
Short-container-title:

Author:

Al-Wahaibi Lamya H.¹,Blacque Olivier²,Al-Shaalan Nora H.¹,Tiekink Edward R. T.³,El-Emam Ali A.⁴^ORCID

Affiliation:

1. Department of Chemistry, College of Sciences , Princess Nourah bint Abdulrahman University , Riyadh 11671 , Saudi Arabia

2. Department of Chemistry , University of Zurich , Winterthurerstrasse 190, 8057 Zurich , Switzerland

3. Research Centre for Crystalline Materials, School of Medical and Life Sciences, Sunway University , 47500 Bandar Sunway , Selangor Darul Ehsan , Malaysia

4. Department of Medicinal Chemistry, Faculty of Pharmacy , Mansoura University , Mansoura 35516 , Egypt

Abstract

Abstract C20H22N4OS, triclinic, P 1 ‾

$P\overline{1}$

(no. 2), a = 6.8528(3) Å, b = 11.3498(5) Å, c = 13.3896(9) Å, α = 114.083(5)°, β = 104.326(4)°, γ = 90.369(3)°, V = 914.38(9) Å3, Z = 2, R gt (F) = 0.0844, wR ref (F 2) = 0.2217, T = 160 K.

Publisher

Walter de Gruyter GmbH

Subject

Inorganic Chemistry,Condensed Matter Physics,General Materials Science

Link

https://www.degruyter.com/document/doi/10.1515/ncrs-2022-0511/pdf

Reference15 articles.

1. Rigaku Oxford Diffraction. CrysAlisPRO; Rigaku Corporation: Oxford, UK, 2019.

2. Sheldrick, G. M. A short history of Shelx. Acta Crystallogr. 2008, A64, 112–122; https://doi.org/10.1107/s0108767307043930.

3. Sheldrick, G. M. Crystal structure refinement with Shelxl. Acta Crystallogr. 2015, C71, 3–8; https://doi.org/10.1107/s2053229614024218.

4. Dolomanov, O. V., Bourhis, L. J., Gildea, R. J., Howard, J. A. K., Puschmann, H. Olex2: a complete structure solution, refinement and analysis program. J. Appl. Crystallogr. 2009, 42, 339–341; https://doi.org/10.1107/s0021889808042726.

5. El-Emam, A. A., Al-Deeb, O. A., Al-Omar, M., Lehmann, J. Synthesis, antimicrobial, and anti-HIV-1 activity of certain 5-(1-adamantyl)-2-substituted thio-1,3,4-oxadiazoles and 5-(1-adamantyl)-3-substituted aminomethyl-1,3,4-oxadiazoline-2-thiones. Bioorg. Med. Chem. 2004, 12, 5107–5013; https://doi.org/10.1016/j.bmc.2004.07.033.