Crystal structure of (3S,8R,10R,12R,14R)-12-hydroxy-4,4,8,10,14-pentamethyl-17-((R)-2,6,6-trimethyltetrahydro-2H-pyran-2-yl) hexadecahydro-1H-cyclopenta[a]phenanthren-3-yl acetate, C32H54O4-Reference-Cited by-同舟云学术

Crystal structure of (3S,8R,10R,12R,14R)-12-hydroxy-4,4,8,10,14-pentamethyl-17-((R)-2,6,6-trimethyltetrahydro-2H-pyran-2-yl) hexadecahydro-1H-cyclopenta[a]phenanthren-3-yl acetate, C32H54O4

Published:2020-10-12 Issue:1 Volume:236 Page:163-166
ISSN:2197-4578
Container-title:Zeitschrift für Kristallographie - New Crystal Structures
language:en
Short-container-title:

Author:

Ma Ying¹^ORCID,Wang Hui-Yun²,Zhang Xiao-Fan¹,Zhao Feng-Lan¹,Meng Qing-Guo¹

Affiliation:

1. School of Pharmacy, Collaborative Innovation Center of Advanced Drug Delivery System and Biotech Drugs in Universities of Shandong, Key Laboratory of Molecular Pharmacology and Drug Evaluation (Yantai University), Ministry of Education , Yantai University , Yantai , PR China

2. College of Pharmacy , Jining Medical University , Rizhao , 276826, PR China

Abstract

Abstract C32H54O4, monoclinic, P21 (no. 4), a = 7.8727(1) Å, b = 19.9173(2) Å, c = 19.1801(2) Å, β = 94.539(1)°, V = 2998.06(6) Å3, Z = 4, R gt (F) = 0.0370, wR ref (F 2) = 0.0983, T = 293 K.

Funder

National Natural Science Foundation of China

Publisher

Walter de Gruyter GmbH

Subject

Inorganic Chemistry,Condensed Matter Physics,General Materials Science

Link

https://www.degruyter.com/document/doi/10.1515/ncrs-2020-0311/pdf

Reference13 articles.

1. Rigaku Oxford Diffracion. CrysAlisPRO software system, version 1.171.39.32a; Rigaku Corporation: Oxford, UK, 2017.

2. Dolomanov, O. V., Bourhis, L. J., Gildea, R. J., Howard, J. A. K., Puschmann, H. OLEX2: a complete structure solution, refinement and analysis program. J. Appl. Crystallogr. 2009, 42, 339–341; https://doi.org/10.1107/s0021889808042726.

3. Sheldrick, G. M. Crystal structure refinement with SHELXL. Acta Crystallogr. 2015, C71, 3–8; https://doi.org/10.1107/s2053229614024218.

4. Palatinus, L., Chapuis, G. SUPERFLIP: a computer program for the solution of crystal structures by charge flipping in arbitrary dimensions. J. Appl. Cryst. 2007, 40, 786–790; https://doi.org/10.1107/s0021889807029238.

5. Liu, J., Xu, Y. R., Yang, J. J., Wang, W. Z., Zhang, J. Q., Zhang, R. M., Meng, Q. G. Discovery, semisynthesis, biological activities, and metabolism of ocotillol-type saponins. J. Ginseng Res. 2017, 41, 373–378; https://doi.org/10.1016/j.jgr.2017.01.001.

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