The crystal structure of 1-ethyl-2-nitro-imidazole oxide, C<sub>5</sub>H<sub>7</sub>N<sub>3</sub>O<sub>3</sub>-Reference-Cited by-同舟云学术

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The crystal structure of 1-ethyl-2-nitro-imidazole oxide, C₅H₇N₃O₃

Published:2023-05-11 Issue:4 Volume:238 Page:743-744
ISSN:1433-7266
Container-title:Zeitschrift für Kristallographie - New Crystal Structures
language:en
Short-container-title:

Author:

Jun Yuan¹,Bingheng Wu²,Yong Wang²,Jianlong Wang³,Duanlin Cao³,Lizhen Chen³

Affiliation:

1. Shanxi College of Technology , Shuozhou 036000 , Shanxi , P. R. China

2. North University of China , Taiyuan , 030051 , Shanxi , P.R. China

3. School of Chemistry and Chemical Engineering, North University of China , Taiyuan , 030051 , Shanxi , P.R. China

Abstract

Abstract C5H7N3O3, monoclinic, P21/n (no. 14), a = 8.7821(7) Å, b = 7.1320(5) Å, c = 11.6293(10) Å, β = 104.718 ( 3 ) ∘

$104.718{(3)}^{\circ }$

, V = 704.49(10) Å3, Z = 4, R g t

${R}_{gt}$

(F) = 0.0468, w R r e f

$w{R}_{ref}$

(F 2) = 0.1125, T = 170.0 K.

Publisher

Walter de Gruyter GmbH

Subject

Inorganic Chemistry,Condensed Matter Physics,General Materials Science

Link

https://www.degruyter.com/document/doi/10.1515/ncrs-2023-0182/pdf

Reference9 articles.

1. BRUKER. SAINT, APEX2 and SADABS. Bruker AXS Inc. Madison, Wisconsin, USA, 2009.

2. Dolomanov, O. V., Bourhis, L. J., Gildea, R. J., Howard, J. A. K., Puschmann, H. OLEX2: a complete structure solution, refinement and analysis program. J. Appl. Cryst. 2009, 42, 339–341; https://doi.org/10.1107/s0021889808042726.

3. Sheldrick, G. M. Crystal structure refinement with SHELXL. Acta Cryst. 2015, C71, 3–8; https://doi.org/10.1107/s2053229614024218.

4. Sheldrick, G. M. A short history of SHELX. Acta Cryst. 2008, A64, 112–122; https://doi.org/10.1107/s0108767307043930.

5. Nunn, A., Linder, K., Strauss, H. W. Nitroimidazoles and imaging hypoxia. Eur. J. Nucl. Med. 1995, 22, 265–280; https://doi.org/10.1007/bf01081524.

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