Crystal structure of 6,7-difluoro-1-methyl-3-(trifluoromethyl)quinoxalin-2(1H)-one, C10H5F5N2O-Reference-Cited by-同舟云学术

Crystal structure of 6,7-difluoro-1-methyl-3-(trifluoromethyl)quinoxalin-2(1H)-one, C10H5F5N2O

Published:2020-12-10 Issue:2 Volume:236 Page:377-378
ISSN:2197-4578
Container-title:Zeitschrift für Kristallographie - New Crystal Structures
language:en
Short-container-title:

Author:

Mi Xia¹^ORCID,Hou Xuehui²,Cui Beibei¹

Affiliation:

1. Henan University of Chinese Medicine , Zhengzhou 450046 , P. R. China

2. Henan University of Animal Husbandry and Economy , Zhengzhou 450000 , P. R. China

Abstract

Abstract C10H5F5N2O, monoclinic, P21/c (no. 14), a = 9.3018(2) Å, b = 25.1396(7) Å, c = 8.9439(2) Å, β = 102.005(3)°, V = 2045.72(10) Å3, Z = 8, R gt(F) = 0.0458, wR ref(F 2) = 0.1345, T = 293(2) K.

Funder

National Natural Science Foundation of China

Education Department of Henan Province

Henan University of Chinese Medicine

Publisher

Walter de Gruyter GmbH

Subject

Inorganic Chemistry,Condensed Matter Physics,General Materials Science

Link

https://www.degruyter.com/document/doi/10.1515/ncrs-2020-0553/pdf

Reference11 articles.

1. Agilent Technologies. CrysAlisPro Software System; Agilent Technologies UK Ltd: Oxford, UK, 2017.

2. Dolomanov, O. V., Bourhis, L. J., Gildea, R. J., Howard, J. A. K., Puschmann, H. OLEX2: a complete structure solution, refinement and analysis program. J. Appl. Crystallogr. 2009, 42, 339–341; https://doi.org/10.1107/s0021889808042726.

3. Sheldrick, G. M. A short history of SHELX. Acta Crystallogr. 2008, A64, 112–122; https://doi.org/10.1107/s0108767307043930.

4. Sheldrick, G. M. Crystal structure refinement with SHELXL. Acta Crystallogr. 2015, C71, 3–8; https://doi.org/10.1107/s2053229614024218.

5. Aoki, K., Koseki, J., Tskeda, S., Aburada, M., Miyamoto, K. Convenient synthetic method for 3-(3-substituted indol-2-yl)quinoxalin-2-ones as VEGF inhibitor. Chem. Pharm. Bull. 2007, 55, 922–925; https://doi.org/10.1248/cpb.55.922.