The crystal structure of 1-(3-oxo-1-phenyl-3-(p-tolyl) propylidene)-1,3-dihydro-2H-inden-2-one, C25H20O2-Reference-Cited by-同舟云学术

The crystal structure of 1-(3-oxo-1-phenyl-3-(p-tolyl) propylidene)-1,3-dihydro-2H-inden-2-one, C₂₅H₂₀O₂

Published:2023-11-08 Issue:1 Volume:239 Page:23-24
ISSN:1433-7266
Container-title:Zeitschrift für Kristallographie - New Crystal Structures
language:en
Short-container-title:

Author:

Wang Mengdan¹^ORCID,Lu Weiwei¹,Wang Junling¹^ORCID,Li Mengyang¹,Feng Yuanyuan¹,Ma Jun-Ying²

Affiliation:

1. School of Chemistry and Chemical Engineering , Henan University of Science and Technology , Luoyang , Henan 471003 , P.R. China

2. School of Chemistry and Chemical Engineering , Henan University of Science and Technology, Provincial and Ministerial Co-construction of Collaborative Innovation Center for Non-ferrous Metal New Materials and Advanced Processing Technology , Luoyang , Henan 471003 , P.R. China

Abstract

Abstract C25H20O2, triclininc, P 1 ‾

$\overline{1}$

(no. 2), a = 9.821(2) Å, b = 10.141(2) Å, c = 10.679(2) Å, α = 61.688(4)°, β = 86.002(4)°, γ = 84.220(4)°, V = 931.3(3) Å3, Z = 2, R gt (F) = 0.0522, wR ref (F 2) = 0.1437, T = 293 K.

Publisher

Walter de Gruyter GmbH

Subject

Inorganic Chemistry,Condensed Matter Physics,General Materials Science

Link

https://www.degruyter.com/document/doi/10.1515/ncrs-2023-0418/pdf

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3. Sheldrick, G. M. SHELXTL – integrated space-group and crystal-structure determination. Acta Crystallogr. 2015, A71, 3–8; https://doi.org/10.1107/s2053273314026370.

4. Sheldrick, G. M. Crystal structure refinement with SHELXL. Acta Crystallogr. 2015, C71, 3–8; https://doi.org/10.1107/s2053229614024218.

5. Muzart, J. One-pot syntheses of α,β-unsaturated carbonyl compounds through palladium-mediated dehydrogenation of ketones, aldehydes, esters, lactones and amides. Eur. J. Org Chem. 2010, 2010, 3779–3790; https://doi.org/10.1002/ejoc.201000278.

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