The crystal structure of 2,8-diethyl-1,3,7,9-tetramethyl-4λ4,5λ4-spiro[dipyrrolo[1,2-c:2′,1′-f][1,3,2]diazaborinine-5,2′-naphtho[1,8-de][1,3,2]dioxaborinine], C25H29BN2O2-Reference-Cited by-同舟云学术

The crystal structure of 2,8-diethyl-1,3,7,9-tetramethyl-4λ⁴,5λ⁴-spiro[dipyrrolo[1,2-c:2′,1′-f][1,3,2]diazaborinine-5,2′-naphtho[1,8-de][1,3,2]dioxaborinine], C₂₅H₂₉BN₂O₂

Published:2024-04-15 Issue:3 Volume:239 Page:477-479
ISSN:1433-7266
Container-title:Zeitschrift für Kristallographie - New Crystal Structures
language:en
Short-container-title:

Author:

Al-Hazmi Ghaferah H.¹,Refat Moamen S.²,Usman Rabia³^ORCID,Khan Arshad⁴^ORCID

Affiliation:

1. Department of Chemistry , College of Science, Princess Nourah bint Abdulrahman University , P.O. Box 84428 , Riyadh 11671 , Saudi Arabia

2. Department of Chemistry , College of Science, Taif University , P.O. Box 11099 , Taif 21944 , Saudi Arabia

3. School of Chemistry and Environmental Engineering , Sichuan University of Science & Engineering , Zigong , Sichuan 643000 , China

4. Nanomedicine Department , King Abdullah International Medical Research Center (KAIMRC), King Saud Bin Abdulaziz University for Health Sciences, Ministry of National Guard Health Affairs , Riyadh 11426 , Kingdom of Saudi Arabia

Abstract

Abstract C25H29BN2O2, monoclinic, P21/c (no. 14), a = 13.1591(3) Å, b = 13.9362(3) Å, c = 13.0463(3) Å, β = 112.066(3)°, V = 2217.29(10) Å3, Z = 4, R gt (F) = 0.0419, wR ref (F 2) = 0.1068, T = 150 K.

Publisher

Walter de Gruyter GmbH

Link

https://www.degruyter.com/document/doi/10.1515/ncrs-2024-0053/pdf

Reference16 articles.

1. Rigaku, O. D. CRYSALISPRO; Rigaku Oxford Diffraction Ltd: Yarnton, Oxfordshire, England, 2015.

2. Sheldrick, G. M. Crystal structure refinement with SHELXL. Acta Crystallogr. 2015, C71, 3–8; https://doi.org/10.1107/s2053229614024218.

3. Sheldrick, G. M. A short history of SHELX. Acta Crystallogr. 2008, A64, 112–122; https://doi.org/10.1107/s0108767307043930.

4. Dolomanov, O. V., Bourhis, L. J., Gildea, R. J., Howard, J. A. K., Puschmann, H. OLEX2: a complete structure solution, refinement and analysis program. J. Appl. Crystallogr. 2009, 42, 339–341; https://doi.org/10.1107/s0021889808042726.

5. Shipalova, M., Bobrov, A., Usoltsev, S., Marfin, Y. S., Rumyantsev, E. Influence of structure and solvatation on photophysical characteristics of meso-substituted boron dipyrrins in solution and bulk hybrid materials. J. Mol. Liq. 2019, 283, 688–694; https://doi.org/10.1016/j.molliq.2019.03.099.