Synthesis and crystal structure of (1E,2E)-3-(anthracen-9-yl)-1-(4-methoxyphenyl)prop-2-en-1-one oxime, C24H19NO2

Author:

Usman Rabia1,Khan Arshad12ORCID,Al-Hazmi Ghaferah H.3,Refat Moamen S.4,He Nongyue1

Affiliation:

1. State Key Laboratory of Bioelectronics, National Demonstration Center for Experimental Biomedical Engineering Education, Southeast University , Nanjing 210096 , P. R. China

2. School of Materials Science and Engineering , Hunan University , Changsha 110016, P. R. China

3. Department of Chemistry , College of Science, Princess Nourah bint Abdulrahman University , Riyadh 11671 , KSA

4. Department of Chemistry , College of Science, Taif University , P. O. Box 11099 , Taif 21944 , Saudi Arabia

Abstract

Abstract C24H19NO2, triclinic, P 1 $P‾{1}$ (no. 2), a = 8.3580(17) Å, b = 10.220(2) Å, c = 11.227(2) Å, α = 85.25(3), β = 81.35(3), γ = 88.72(3), V = 944.8(3) Å3, Z = 2, R gt (F) = 0.0873, wR ref (F 2) = 0.1988, T = 293 K.

Publisher

Walter de Gruyter GmbH

Subject

Inorganic Chemistry,Condensed Matter Physics,General Materials Science

Reference11 articles.

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3. Sheldrick, G. M. Crystal structure refinement with Shelxl. Acta Crystallogr. 2015, C71, 3–8; https://doi.org/10.1107/s2053229614024218.

4. Brandenburg, K. DIAMOND. Visual Crystal Structure Information System. Ver. 4.0; Crystal Impact: Bonn, Germany, 2015.

5. Xu, X., Li, J., Du, C., Song, Y. Improved synthesis of 1,3-diaryl-2-propen-1-one oxime in the presence of anhydrous sodium sulfate. Chin. J. Chem. 2011, 29, 2781–2784; https://doi.org/10.1002/cjoc.201100038.

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