The crystal structure of (Z)-4-ethyl-2-((4-ethyl-3,5-dimethyl-1H-pyrrol-2-yl)methylene)-3,5-dimethyl-2H-pyrrol-1-ium 2,2'-spirobi[naphtho[1,8-de][1,3,2]dioxaborinin]-2-uide, C37H37BN2O4-Reference-Cited by-同舟云学术

The crystal structure of (Z)-4-ethyl-2-((4-ethyl-3,5-dimethyl-1H-pyrrol-2-yl)methylene)-3,5-dimethyl-2H-pyrrol-1-ium 2,2'-spirobi[naphtho[1,8-de][1,3,2]dioxaborinin]-2-uide, C₃₇H₃₇BN₂O₄

Published:2024-04-04 Issue:3 Volume:239 Page:503-505
ISSN:1433-7266
Container-title:Zeitschrift für Kristallographie - New Crystal Structures
language:en
Short-container-title:

Author:

Alsuhaibani Amnah Mohammed¹,Asiri Yazeed M.²,Refat Moamen S.²,Usman Rabia³^ORCID,Khan Arshad⁴^ORCID

Affiliation:

1. Department of Physical Sports Sciences, College of Sports Sciences & Physical Activity , Princess Nourah bint Abdulrahman University , P. O. Box 84428 , Riyadh 11671 , Saudi Arabia

2. Department of Chemistry, College of Science , Taif University , P. O. Box 11099 , 21944 Taif , Saudi Arabia

3. School of Chemistry and Environmental Engineering , Sichuan University of Science & Engineering , Zigong , Sichuan 643000 , China

4. Nanomedicine Department, King Abdullah International Medical Research Center (KAIMRC), King Saud Bin Abdulaziz University for Health Sciences , Ministry of National Guard Health Affairs , Riyadh 11426 , Kingdom of Saudi Arabia

Abstract

Abstract C37H37BN2O4, monoclinic, I2/a (no. 15), a = 13.8030(3) Å, b = 17.6109(2) Å, c = 14.1059(3) Å, β = 117.524(3)°, V = 3040.83(11) Å3, Z = 4, Rgt (F) = 0.0340, wRref (F 2) = 0.0867, T = 150 K.

Funder

Princess Nourah bint Abdulrahman University

King Abdullah International Medical Research Center

Publisher

Walter de Gruyter GmbH

Link

https://www.degruyter.com/document/doi/10.1515/ncrs-2024-0063/pdf

Reference20 articles.

1. Rigaku O. D. CrysAlisPRO; Rigaku Oxford Diffraction Ltd: Yarnton, Oxfordshire, England, 2015.

2. Sheldrick, G. M. Crystal structure refinement with SHELXL. Acta Crystallogr. 2015, C71, 3–8; https://doi.org/10.1107/s2053229614024218.

3. Sheldrick, G. M. A short history of SHELX. Acta Crystallogr. 2008, A64, 112–122; https://doi.org/10.1107/s0108767307043930.

4. Dolomanov, O. V., Bourhis, L. J., Gildea, R. J., Howard, J. A. K., Puschmann, H. OLEX2: a complete structure solution, refinement and analysis program. J. Appl. Crystallogr. 2009, 42, 339–341; https://doi.org/10.1107/s0021889808042726.

5. Desiraju, G. R. Supramolecular synthons in crystal engineering? A new organic synthesis. Angew. Chem. Int. Ed. 1995, 34, 2311–2327; https://doi.org/10.1002/anie.199523111.