Crystal structure of diethyl 4,6-diphenyl-1,9-di-p-tolylhexahydro-3H-2,7,3,5-(epimethanetriyliminomethanetriyl)cyclopenta[b]pyridine-3,5(2H)-dicarboxylate, C42H42N2O4-Reference-Cited by-同舟云学术

Crystal structure of diethyl 4,6-diphenyl-1,9-di-p-tolylhexahydro-3H-2,7,3,5-(epimethanetriyliminomethanetriyl)cyclopenta[b]pyridine-3,5(2H)-dicarboxylate, C₄₂H₄₂N₂O₄

Published:2022-04-04 Issue:3 Volume:237 Page:455-457
ISSN:1433-7266
Container-title:Zeitschrift für Kristallographie - New Crystal Structures
language:en
Short-container-title:

Author:

Fan Shuai¹,Zhang Qian¹,Lv Xu-Dong¹,Jin Yuan-Yuan¹,Yang Zhao-Yong¹

Affiliation:

1. Institute of Medicinal Biotechnology, Chinese Academy of Medical Sciences & Peking Union Medical College , Tiantanxili, 100050 Beijing , P. R. China

Abstract

Abstract C42H42N2O4, triclinic, P 1 ‾

$P\overline{1}$

(no. 2), a = 9.309(3) Å, b = 14.191(5) Å, c = 14.918(5) Å, α = 69.221(4)°, β = 82.384(5)°, γ = 72.805(4)°, V = 1759.3(10) Å3, Z = 2, R gt (F) = 0.0699, wR ref (F 2) = 0.1806, T = 296 K.

Publisher

Walter de Gruyter GmbH

Subject

Inorganic Chemistry,Condensed Matter Physics,General Materials Science

Link

https://www.degruyter.com/document/doi/10.1515/ncrs-2022-0029/pdf

Reference8 articles.

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3. Sheldrick, G. M. A short history of SHELX. Acta Crystallogr. 2008, A64, 112–122; https://doi.org/10.1107/s0108767307043930.

4. Wan, J. P., Lin, Y. F., Jing, Y. F. Selectivity tunable divergent synthesis of 1,4-and 1,2-dihydropyridines via three-component reactions. Tetrahedron 2014, 70, 7874–7880; https://doi.org/10.1016/j.tet.2014.09.002.

5. Hilgeroth, A., Baumeister, U., Heinemann, F. W. Solution dimerization of 4-ary-1,4-dihydropyridines. Eur. J. Org Chem. 2000, 2000, 245–249; https://doi.org/10.1002/(sici)1099-0690(200001)2000:2<245::aid-ejoc245>3.0.co;2-2.

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