The crystal structure of 3-(2-bromophenyl)-1,5-di-p-tolylpentane-1,5-dione, C25H23BrO2-Reference-Cited by-同舟云学术

The crystal structure of 3-(2-bromophenyl)-1,5-di-p-tolylpentane-1,5-dione, C₂₅H₂₃BrO₂

Published:2022-07-04 Issue:5 Volume:237 Page:829-831
ISSN:1433-7266
Container-title:Zeitschrift für Kristallographie - New Crystal Structures
language:en
Short-container-title:

Author:

Liu Wanxing¹,Dai Yifan²,Shen Guodong²^ORCID

Affiliation:

1. The Non-Public Enterprise Service Center of Liaocheng , School of Chemistry and Chemical Engineering Liaocheng University , Liaocheng 252000 , Shandong , China

2. School of Chemistry and Chemical Engineering Liaocheng University , Liaocheng 252000 , Shandong , China

Abstract

Abstract C25H23BrO2, monoclinic, P21/c (no. 14), a = 9.6229(7) Å, b = 21.7953(16) Å, c = 10.9104(6) Å, β = 109.330(7)°, V = 2159.3(3) Å3, Z = 4, R gt (F) = 0.0499, wR ref (F 2) = 0.1385, T = 293 K.

Publisher

Walter de Gruyter GmbH

Subject

Inorganic Chemistry,Condensed Matter Physics,General Materials Science

Link

https://www.degruyter.com/document/doi/10.1515/ncrs-2022-0250/pdf

Reference13 articles.

1. Oxford Diffraction Ltd. CrysAlisPRO, version 1.171.41.121a; Rigaku Oxford Diffraction: England, 2021.

2. Sheldrick, G. M. SHELXTL – integrated space-group and crystal-structure determination. Acta Crystallogr. 2015, A71, 3–8; https://doi.org/10.1107/s2053273314026370.

3. Sheldrick, G. M. Crystal structure refinement with SHELXL. Acta Crystallogr. 2015, C71, 3–8; https://doi.org/10.1107/s2053229614024218.

4. Sodhi, R. K., Paul, S., Gupta, V. K., Kant, R. Conversion of /a, /b-unsaturated ketones to 1,5-diones via tandem retro–Aldol and Michael addition using Co(acac)2 covalently anchored onto amine functionalized silica. Tetrahedron Lett. 2015, 56, 1944–1948; https://doi.org/10.1016/j.tetlet.2015.02.057.

5. Yan, Y., Yang, J., Yu, Z., Yu, M., Ma, Y.-T., Wang, L., Su, C., Luo, J., Horsman, G. P., Huang, S.-X. Non-enzymatic pyridine ring formation in the biosynthesis of the rubrolone tropolone alkaloids. Nat. Commun. 2016, 7, 13083; https://doi.org/10.1038/ncomms13083.