Crystal structure of 4-chloro-N′-[(1E)-(2-nitrophenyl)methylidene]benzohydrazide, C14H10ClN3O3-Reference-Cited by-同舟云学术

Crystal structure of 4-chloro-N′-[(1E)-(2-nitrophenyl)methylidene]benzohydrazide, C₁₄H₁₀ClN₃O₃

Published:2023-04-27 Issue:4 Volume:238 Page:631-633
ISSN:1433-7266
Container-title:Zeitschrift für Kristallographie - New Crystal Structures
language:en
Short-container-title:

Author:

Al-Wahaibi Lamya H.¹,Blacque Olivier²,Tiekink Edward R. T.³,El-Emam Ali A.⁴^ORCID

Affiliation:

1. Department of Chemistry, College of Sciences , Princess Nourah bint Abdulrahman University , Riyadh 11671 , Saudi Arabia

2. Department of Chemistry , University of Zurich , Winterthurerstrasse 190 , 8057 Zurich , Switzerland

3. Research Centre for Crystalline Materials, School of Medical and Life Sciences , Sunway University , 47500 Bandar Sunway , Selangor Darul Ehsan , Malaysia

4. Department of Medicinal Chemistry, Faculty of Pharmacy , Mansoura University , Mansoura 35516 , Egypt

Abstract

Abstract C14H10ClN3O3, triclinic, P1 (no. 1), a = 4.8813(2) Å, b = 6.7806(2) Å, c = 10.3135(2) Å, α = 98.101 ( 2 ) ∘

$98.101{\left(2\right)}^{\circ }$

, β = 94.174 ( 2 ) ∘

$94.174{\left(2\right)}^{\circ }$

, γ = 97.612 ( 3 ) ∘

$97.612{\left(3\right)}^{\circ }$

, V = 333.515(18) Å3, Z = 1, R g t

${R}_{gt}$

(F) = 0.0270, w R r e f

$w{R}_{ref}$

(F2) = 0.0743, T = 160 K.

Funder

Princess Nourah bint Abdulrahman University, Riyadh, Saudi Arabia

Publisher

Walter de Gruyter GmbH

Subject

Inorganic Chemistry,Condensed Matter Physics,General Materials Science

Link

https://www.degruyter.com/document/doi/10.1515/ncrs-2023-0125/pdf

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3. Sheldrick, G. M. Crystal structure refinement with SHELXL. Acta Crystallogr. 2015, C71, 3–8; https://doi.org/10.1107/s2053229614024218.

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5. Yu, W., Huang, G., Zhang, Y., Liu, H., Dong, L., Yu, X., Li, Y., Chang, J. I2-Mediated oxidative C–O bond formation for the synthesis of 1,3,4-oxadiazoles from aldehydes and hydrazides. J. Org. Chem. 2013, 78, 10337–10343; https://doi.org/10.1021/jo401751h.

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