The crystal structure of fac-tricarbonyl(2-pyridin-2-yl-quinoline-κ2 N,N′)-(pyrazole-κN)rhenium(I)nitrate, C20H14N4O3ReNO3-Reference-Cited by-同舟云学术

The crystal structure of fac-tricarbonyl(2-pyridin-2-yl-quinoline-κ² N,N′)-(pyrazole-κN)rhenium(I)nitrate, C₂₀H₁₄N₄O₃ReNO₃

Author:

Sithole Sibusiso A.¹^ORCID,Malan Federick P.²^ORCID,Katerere David R.³,Manicum Amanda-Lee E.¹^ORCID

Affiliation:

1. Department of Chemistry , Tshwane University of Technology , Pretoria 0001 , South Africa

2. Department of Chemistry , University of Pretoria , Pretoria 0028 , South Africa

3. Department of Pharmaceutical Sciences , Tshwane University of Technology , Pretoria 0001 , South Africa

Abstract

Abstract C 20 H 14 N 4 O 3

${\mathrm{C}}_{20}{\mathrm{H}}_{14}{\mathrm{N}}_{4}{\mathrm{O}}_{3}$

Re N O 3

${\mathrm{N}\mathrm{O}}_{3}$

, monoclinic, P 2 1

${2}_{1}$

/c (no. 14), a = 12.9572 (2), b = 9.1568 (2), c = 17.3658 (3) Å, β = 97.267 ( 2 ) °

$97.267(2){}^{\circ}$

, V = 2043.84 (7)  Å 3

${\mathrm{\mathring{\text{A}}}}^{3}$

, Z = 4, R g t

${R}_{gt}$

(F) = 0.0231, w R r e f

$w{R}_{ref}$

( F 2

${F}^{2}$

) = 0.0514, T = 154 K

Funder

National Research Foundation

Tshwane University of Technology

University of Pretoria

Publisher

Walter de Gruyter GmbH

Subject

Inorganic Chemistry,Condensed Matter Physics,General Materials Science

Link

Reference16 articles.

1. System, C. S. CrysAlis Pro Software System; Rigaku Oxford Diffraction: Yarnton, UK, 2021.

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